Qiji Chemical
Products

Tetrabutylammonium Bromide

Qiji Chemical

Tetrabutylammonium Bromide
Specifications

HS Code

620201

Chemical Formula C16H36BrN
Molar Mass 322.37 g/mol
Appearance White crystalline solid
Odor Odorless
Melting Point 103 - 104 °C
Boiling Point Decomposes
Solubility In Water Soluble
Solubility In Organic Solvents Soluble in many organic solvents like ethanol, acetone
Density 1.039 g/cm³ (20 °C)
Ph Aqueous Solution Neutral
Cas Number 1643-19-2
Packing & Storage
Packing 500g of Tetrabutylammonium Bromide in a sealed, chemical - resistant plastic bag.
Storage Tetrabutylammonium bromide should be stored in a cool, dry place away from heat and ignition sources. Keep it in a tightly - sealed container to prevent moisture absorption and contamination. Store separately from oxidizing agents and incompatible substances. Ideal storage conditions help maintain its chemical stability and prevent potential reactions or degradation.
Shipping Tetrabutylammonium Bromide is shipped in sealed, corrosion - resistant containers. Adequate cushioning ensures protection during transit. Shipment follows strict chemical transport regulations to prevent leakage and ensure safety.
Free Quote

For samples, pricing, or more information, please call us at +8615371019725 or mail to info@bouling-chem.com.

We will respond to you as soon as possible.

Tel: +8615371019725

Email: info@bouling-chem.com

Tetrabutylammonium Bromide Tetrabutylammonium Bromide
General Information
Historical Development
"The History of Tetrabutylammonium Bromide"
Tetrabutylammonium bromide is one of the most eye-catching substances in chemistry. Looking back to the past, its initial appearance was not deeply studied by the academic community, and it was only a glimmer on the path of chemical exploration.
At that time, people knew very little about its properties and uses. However, scientific researchers did not give up studying, and over the years, their understanding of it gradually increased. Since the beginning, only its basic composition was known, and its excellent function in phase transfer catalysis was later understood, which was actually one of the great advances in the development of chemistry.
With the passage of time, the experimental methods became more and more exquisite, and the research on tetrabutylammonium bromide became more and more in-depth. In the field of organic synthesis, it has gradually become an indispensable auxiliary agent, helping many complex reactions to progress smoothly. From initial exploration to wide application, this is the evidence of the spirit of scientific exploration, and it is also the brilliant track of the development of tetrabutylammonium bromide.
Product Overview
Tetrabutylammonium bromide is also a chemical substance. Its shape is like powder, and its color is white and shiny. This agent is often used as a phase transfer catalyst in the field of organic synthesis, which can promote the speed of reaction and increase the yield. Its mild nature is mostly suitable for various reaction systems.
Preparation method, or bromobutane and trimethylamine as materials, obtained by reaction. In industry and scientific research, it has a wide range of uses. It can be used to prepare special organic compounds, and it also plays a key role in the manufacture of some fine chemicals. And in the phase transfer catalytic reaction, it has unique properties, making many reactions easy to carry out. It is an indispensable substance for chemical research and production.
Physical & Chemical Properties
Tetrabutylammonium bromide is also a chemical product. Its properties have physical and chemical characteristics. Looking at its physics, it is white and crystalline at room temperature, resembling a fine salt, and is easily soluble in water, alcohol and other solvents, with good solubility, which is convenient for it to be evenly dispersed in various reaction systems.
In terms of its chemical properties, tetrabutylammonium bromide is a quaternary ammonium salt and has a certain chemical activity. In many organic synthesis reactions, it is often used as a phase transfer catalyst, which can promote the reaction to proceed efficiently between two phases. Due to its structure, the ammonium ion part can interact with the anion, thereby changing the hydrophilicity and lipophilicity of the substance, so that the reactants that were originally difficult to contact can effectively react, improve the reaction rate and yield, and are widely used in the field of organic chemical synthesis.
Technical Specifications & Labeling
Today there is a product name Tetrabutylammonium Bromide, and its process specifications and identification (product parameters) are the key. The process of this product needs to be carefully researched to control its synthesis process. The ratio of raw materials is accurate, and the reaction conditions need to be strictly inspected. Temperature, pressure, etc. should not be ignored, so that the reaction is smooth and the product is pure.
In terms of its identification, the product parameters should be clear and correct, from the standard of purity to the description of characteristics, all should be detailed. The purity needs to be of the highest quality, and the impurity content is minimal. The characterization of properties must be accurate, and color, shape, etc. are all important. In this way, the essence of the Tetrabutylammonium Bromide process and identification can be obtained to meet all needs and meet the research requirements.
Preparation Method
The method of making tetrabutylammonium bromide is made of sodium bromide and bromobutane as raw materials. The preparation process involves first taking an appropriate amount of sodium bromide, dissolving it in a mixed solvent of alcohol and water, and then slowly adding bromobutane. Heat should be applied, and the temperature should be controlled in a specific range. During this period, it must be stirred frequently to promote the uniform reaction.
The reaction steps proceed in an orderly manner. At the beginning, the two meet and gradually change in combination. As the reaction advances, the properties of the system gradually change. After the reaction is completed, the crude product can be obtained after cooling and separation.
For refining, the method of recrystallization is often used to select a suitable solvent. After dissolving the crude product, heat filtration is used to remove impurities, and then the temperature is lowered to crystallize to obtain pure tetrabutylammonium bromide. The preparation of this preparation requires temperature control and stirring, which is related to the yield and quality.
Chemical Reactions & Modifications
Today there is a chemical substance, named Tetrabutylammonium Bromide. In chemical reactions, its properties are quite critical. Looking at various reactions, this substance is often the main cause of initiation or promotion.
It can optimize the reaction path, just like the wind in a boat, moving forward smoothly. The difficulty of the reaction in the past, it is easy to encounter this. And it can change the properties of the compound, just like a craftsman carving, giving new quality.
Or in the field of phase transfer catalysis, it is like a bridge, connecting different phases, making the reaction speed up. It can also adjust the rate of the reaction, with a certain degree of urgency. Therefore, in chemical research, the reaction and modification of Tetrabutylammonium Bromide are really important for scholars to study, and cannot be ignored.
Synonyms & Product Names
Tetrabutylammonium bromide is also a chemical product. Although its name is the same, it is also known as many. Or tetrabutylammonium bromide, its meaning is the same as tetrabutylammonium bromide. It is also called TBAB, which is the acronym of Tetrabutylammonium Bromide in English, and also refers to this product.
In the market, its product names are also different. Or marked with a unique name, but they are all tetrabutylammonium bromide. Although the names are different, they actually refer to the quality of this chemical. They are all used in chemical, scientific research and other fields, and are commonly used reagents in chemical experiments and production.
Safety & Operational Standards
Tetrabutylammonium bromide is also a chemical agent. During its experiment and application, safety and operating standards are of paramount importance.
This agent has certain chemical activity, and procedures must be followed when handling it. The first protection is to ensure that the experimenter is comprehensive. When holding protective gloves, the material should be able to resist the corrosion of this agent, and prevent it from touching the skin and causing skin damage. Protective glasses should be worn to prevent the agent from splashing in and damaging the eyes. Wear laboratory clothes to isolate the agent and clothing to reduce the risk of pollution.
Furthermore, the operating environment should also be paid attention to. It is suitable for well-ventilated places to avoid the accumulation of volatile gases from the agent, which will cause indoor air pollution and harm the health of the experimenter. If it is operated in a ventilated cabinet, harmful gases can be quickly discharged and the air can be kept fresh.
Tetrabutylammonium bromide should be taken according to accurate measurement. Take it with a clean appliance to avoid impurities from mixing and affecting the quality of the preparation. After use, seal it tightly, and place it in a dry, cool and difficult place for children to prevent it from deteriorating or causing accidents.
If the agent is accidentally spilled during the experiment, do not panic. Clean it up quickly according to the established process. A small amount of spillage can be covered with moisture-absorbing materials, collected carefully, and discarded in the designated container; if a large amount is spilled, when evacuating people, quickly start the ventilation equipment, and professionals will deal with it according to the specifications.
In short, in the operation of tetrabutylammonium bromide, safety must be the priority, and operating standards must be strictly adhered to in order to avoid accidents, ensure the smooth operation of the experiment, and ensure the well-being of personnel.
Application Area
Tetrabutylammonium bromide is very effective in many application fields. In the field of organic synthesis, it is often used as a phase transfer catalyst. Because it can effectively transfer the reactants between two mutually insoluble phases, it can promote the smooth progress of the reaction, speed up the reaction rate and increase the yield. For example, in the reaction of some halogenated hydrocarbons with nucleophiles, it can significantly improve the reaction conditions.
In the field of materials science, it also has its uses. It can participate in the preparation process of specific materials and affect the structure and properties of materials. In the synthesis of some functional materials, tetrabutylammonium bromide can regulate the reaction path, so that the resulting materials have unique properties.
In chemical production, it helps to optimize the production process and improve product quality. In short, tetrabutylammonium bromide plays an important role in the application fields of phase transfer catalysis, material preparation and chemical production, and is of great significance to the development of many fields.
Research & Development
Today there is a chemical substance called tetrabutylammonium bromide (Tetrabutylammonium Bromide). I have dedicated myself to studying this substance for a long time. In the experimental investigation, I have carefully observed its properties and characteristics. Observe the mechanism of its reaction and study the law of its change.
After repeated trials, it is well known that it can be used as a phase transfer catalyst in many chemical reactions, and its effect is remarkable. It can slow down the reaction conditions, improve the reaction rate, and increase its yield.
I hope to further expand its application scope in future research. Or in the synthesis of new materials, or in green chemical processes, I hope it can emerge, contribute to the development of the chemical field, and promote it to a new level, and help the progress and innovation of scientific research.
Toxicity Research
"Study on the toxicity of tetrabutylammonium bromide"
The toxicity of tetrabutylammonium bromide is being studied. Observe its effects on organisms in various experimental situations. Take various organisms as samples to explore the physiological changes after exposure to this agent.
After research, it is found that at high concentrations, it disturbs biological cells or causes cell dysfunction. However, at low concentrations, the effect is not significant.
The toxicity of tetrabutylammonium bromide is related to the dose. Moderate control of its use can reduce its harm to the environment and organisms. To clarify its details, further research is needed to determine the boundaries of its safe use and prevent it from being a disaster to the environment.
Future Prospects
Tetrabutylammonium Bromide is already very important in today's chemical industry. Its use is widely involved in catalysis, helping all reactions to proceed smoothly, and the effect is quite good.
Looking at the future, its development scene can really be expected. Scientists should be more diligent, explore its novelty and expand its use. Or in the field of fine chemicals, it can help create new quality and add wonders to the forest of materials. Or in the path of green chemistry, develop unique capabilities, reduce pollution and harm, and combine the trend of the world.
It is believed that under the study of the sages, Tetrabutylammonium Bromide will be able to shine in the future, making great contributions to the advancement of the chemical industry and the benefit of people's livelihood, and recognizing its extraordinary value.
Frequently Asked Questions
What are the main uses of tetrabutylammonium bromide?
Titanium tetrachloride is an important chemical substance with a wide range of main uses.
In the field of metallurgy, titanium tetrachloride is a key raw material for the preparation of titanium metal. Starting with titanium-containing minerals such as rutile, titanium tetrachloride is prepared by reacting with chlorine gas, and then reduced by magnesium or sodium to obtain high-purity titanium metal. Titanium metal has many excellent characteristics, such as low density, high strength, good corrosion resistance, etc., and is indispensable in aerospace, shipbuilding, chemical equipment and other industries. In aerospace, titanium alloys are often used for aircraft engine parts, fuselage structural parts, etc. In this process, titanium tetrachloride plays an important role as a starting material.
In the chemical industry, titanium tetrachloride also has many uses. First, it can be used as a catalyst. In the polymerization of olefins, titanium tetrachloride is combined with alkyl aluminum and other cocatalysts, which can efficiently catalyze the polymerization of olefins, and prepare polyolefin materials with different properties, such as polyethylene, polypropylene, etc. These polyolefin materials are widely used in the production of plastic products and fibers. Second, titanium tetrachloride can be used to prepare titanium dioxide. Titanium dioxide is a white pigment with excellent performance. It has the advantages of high hiding power and high whiteness. It is widely used in coatings, plastics, papermaking and other industries. Titanium tetrachloride is used as raw material and high-quality titanium dioxide can be prepared by gas phase oxidation and other processes.
In addition, titanium tetrachloride can also be used to prepare other titanium-containing compounds, which are also important in the fields of electronics and ceramics. In the field of electronics, some titanium-containing compounds can be used as electronic ceramic materials, used in capacitors, resistors and other electronic components; in the field of ceramics, the addition of titanium-containing compounds can improve the properties of ceramics, such as improving their strength, toughness and high temperature resistance. In short, titanium tetrachloride plays a pivotal role in many industries and is of great significance in promoting industrial development.
What are the physical properties of tetrabutylammonium bromide?
Ferric oxide is an important oxide of iron, and it has unique physical properties, which is worth studying in detail.
When it comes to color and state, ferric oxide is black and solid, and the texture is quite solid. Its appearance is dark, with a certain metallic luster, which is easy to identify in many scenarios.
Looking at its density, ferric oxide has a higher density and is heavier than common substances at the same volume. This property makes it particularly valuable in some application scenarios where the relationship between the weight and volume of the substance needs to be considered.
Besides its magnetism, ferric oxide is magnetic, which is one of its remarkable characteristics. It can be attracted by magnets and can also exhibit its own magnetism. This magnetic property is widely used in many fields, such as the preparation of magnetic materials, magnetic recording media, etc., and plays a key role.
As for the melting point, ferric oxide has a high melting point and requires a high temperature to melt it. This high melting point characteristic allows ferric oxide to maintain a stable solid-state structure in high-temperature environments, and can be used in refractory materials and other fields.
In addition, ferric oxide is insoluble in water and can remain solid in water, and does not react with water. This property determines that it can maintain its own structure and properties in contact with water, and is not affected by water.
In summary, the black solid form, high density, magnetic properties, high melting point, and insolubility in water of ferric oxide make it indispensable in many fields and lay the foundation for many industrial production, scientific research, and daily life applications.
What are the common functions of tetrabutylammonium bromide in chemical reactions?
Titanium tetrachloride is commonly used in chemical reactions as follows:
First, as a chlorinating agent. In the field of metallurgy, for example, in the extraction process of titanium, rutile (the main component TiO _ 2) is co-heated with coke and chlorine, and titanium tetrachloride is used as a chlorinating agent to participate in the reaction. In this process, TiO _ 2 + 2C + 2Cl _ 2 $\ stackrel {high temperature} {=} $TiCl+ 2CO, titanium tetrachloride is converted from titanium by chlorination reaction, and then further reduced to obtain metal titanium. In organic synthesis, like the chlorination reaction of aromatic side chains, titanium tetrachloride can introduce chlorine atoms into the side chains of aromatics, thereby changing the structure and properties of organic matter.
Second, as a catalyst. It plays a key catalytic role in many reactions in organic synthesis. For example, the famous Friedel-Crafts reaction, whether it is alkylation or acylation reaction, titanium tetrachloride can interact with halogenated hydrocarbons or acyl halides to generate active intermediates such as carbon positive ions, which greatly reduces the reaction activation energy, promotes the smooth reaction of aromatics with halogenated hydrocarbons or acyl halides, realizes the construction of carbon-carbon bonds, and synthesizes a variety of complex organic compounds. In the polymerization of olefins, titanium tetrachloride and alkyl aluminum form a Ziegler-Natta catalyst system, which has high catalytic activity and selectivity for olefin polymerization, and can prepare polyolefin materials with different structures and properties, such as high-density polyethylene, isotactic polypropylene, etc., which is of great significance in the synthesis of polymer materials.
Third, it is called Lewis acid. Due to the empty orbit of the central titanium atom, it can accept electron pairs and exhibit the characteristics of Lewis acid. In some organic reactions, coordination compounds are formed with compounds containing lone pairs of electrons, such as ethers and amines, which change the electron cloud distribution of the reactants and affect the reactivity and selectivity. For example, in some cyclization reactions, titanium tetrachloride coordinates with atoms such as oxygen and nitrogen in the reactant molecules to guide the reaction in a specific direction to generate cyclic compounds with specific structures.
What is the preparation method of tetrabutylammonium bromide?
Titanium tetrachloride is an important chemical raw material. Although the preparation method is not detailed in the ancient book "Tiangong Kaiwu", the method can be studied as follows:
The first rutile chlorination method. This is the rutile (mainly containing titanium dioxide) as raw material, which is mixed with coke and placed in a chlorination furnace. The furnace is filled with chlorine gas, and under high temperature conditions, a chemical reaction occurs. Titanium dioxide in rutile interacts with chlorine gas and coke, and the reaction equation is $TiO_ {2} + 2C + 2Cl_ {2}\ stackrel {high temperature }{=\!=\!=} TiCl_ {4} + 2CO $. In this reaction, coke is used as a reducing agent to reduce titanium dioxide, and chlorine is combined with it to form titanium tetrachloride gas. The generated titanium tetrachloride gas is condensed and collected, and then distilled and purified to obtain high-purity titanium tetrachloride.
Furthermore, it can be prepared from ilmenite. First, ilmenite ($FeTiO_ {3} $) is reacted with sulfuric acid to obtain titanium oxysulfate ($TiOSO_ {4} $) solution. The reaction is as follows: $FeTiO_ {3} + 2H_ {2} SO_ {4} = TiOSO_ {4} + FeSO_ {4} + 2H_ {2} O $. After hydrolysis, titanium sulfate is hydrolyzed to form metatitanic acid ($H_ {2} TiO_ {3} $) precipitation, $TiOSO_ {4} + 2H_ {2} O = H_ {2} TiO_ {3}\ downarrow + H_ {2} SO_ {4} $. The precipitation is calcined to obtain titanium dioxide, $H_ {2} TiO_ {3}\ stackrel {high temperature }{=\!=\!=} {2} + H_ {2} O $TiO_. The obtained titanium dioxide is then reacted with chlorine gas and coke to produce titanium tetrachloride by the rutile chlorination method.
Or the natural rutile and artificial rutile are treated by chlorination method. These materials react directly with chlorine at high temperature and under the action of a catalyst to form titanium tetrachloride. In this process, precise control of reaction temperature, chlorine flow rate and other conditions is crucial, which is related to the yield and purity of titanium tetrachloride. The above preparation methods all need to be strictly operated and follow chemical principles to produce high-quality titanium tetrachloride.
What are the precautions when using tetrabutylammonium bromide?
Titanium tetrachloride is a highly corrosive chemical. When using it, many things must be paid attention to.
First, it is related to protective measures. Users must wear complete protective equipment, such as acid and alkali resistant protective clothing, protective gloves, protective glasses and gas masks. Because of its strong corrosiveness and irritation, if accidentally touched, it will cause serious burns to the skin, eyes and other parts; if inhaled, its volatile aerosol will also cause damage to the respiratory tract.
Second, environmental conditions are extremely critical. The place of use should be well ventilated, and it is best to have a strong ventilation device to quickly disperse the aerosol generated by titanium tetrachloride volatilization and prevent it from accumulating in the air. At the same time, the operation should be carried out in a specific fume hood, which can further ensure the safety of the operator and avoid the spread of aerosol outside the operation area.
Third, the access operation should be cautious. When opening the container containing titanium tetrachloride, the action must be gentle to prevent the container from being damaged and causing it to leak. During the access process, special utensils should be used, such as corrosion-resistant funnels, droppers, etc., and the container should be sealed immediately after access to prevent long-term contact with air and reaction.
Fourth, storage requirements should not be ignored. Titanium tetrachloride should be stored in a dry, cool and ventilated place, away from fire and heat sources, and should be stored separately from alkalis, alcohols and other substances, and must not be mixed. Because it will react violently in contact with water and produce hydrogen chloride gas, the drying of the storage environment is crucial.
Fifth, emergency response must have a plan. In the event of a leak, personnel in the contaminated area should be quickly evacuated to a safe area, quarantined, and access strictly restricted. Emergency personnel must wear protective equipment and respirators, and do not let the leak come into contact with combustible substances. In the case of a small amount of leakage, it can be mixed with sand, dry lime or soda ash; in the case of a large amount of leakage, a dike should be built or a pit should be dug for containment, and relevant departments should be reported in a timely manner and handled by professionals.